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http://hdl.handle.net/11320/16409| Tytuł: | Application of Micellar Extraction for Isolation of Famotidine from Aqueous Samples Prior to its Chromatographic Determination |
| Autorzy: | Kiszkiel-Taudul, Ilona Starczewska, Barbara Karpińska, Joanna Kasabuła, Monika |
| Słowa kluczowe: | Famotidine SDS Triton X-114 Micellar extraction Surface water analysis HPLC–UV |
| Data wydania: | 2017 |
| Data dodania: | 19-kwi-2024 |
| Wydawca: | Springer |
| Źródło: | Journal of Surfactants and Detergents, Volume 20, Issue 6 (2017), p. 1401–1409 |
| Abstrakt: | Micellar extraction was applied to isolate famotidine from aqueous samples. This drug is an H2 receptor antagonist used for the treatment of stomach diseases. The process was performed with a mixture of anionic sodium dodecylsulfate and nonionic Triton X-114 surfactants. The effect of different parameters on the efficiency of the micellar extraction such as electrolyte and surfactant concentration, pH of sample, temperature, shaking and centrifugation time was investigated. The influence of foreign substances on a studied process was tested. The elaborated procedure was applied for HPLC–UV determination of famotidine in natural water samples. The calibration graph was recorded in the range 1.35–37.12 lg mL-1 of the studied compound. The repeatability of the method was equal to 7.4%. The limit of detection and quantification values for the determination of famotidine by using the proposed method amounted to 0.40 and 1.25 lg mL-1 , respectively. |
| Afiliacja: | Ilona Kiszkiel-Taudul - Institute of Chemistry, University of Bialystok, 15-245 Białystok, Poland Barbara Starczewska - Institute of Chemistry, University of Bialystok, 15-245 Białystok, Poland Joanna Karpińska - Institute of Chemistry, University of Bialystok, 15-245 Białystok, Poland Monika Kasabuła - Institute of Chemistry, University of Bialystok, 15-245 Białystok, Poland |
| Nota biograficzna: | Dr. ILONA KISZKIEL-TAUDUL is an academic assistant at Institute of Chemistry (Biological–Chemical Department, University of Bialystok). The performed studies by Dr. Taudul are relative to elaboration of new extraction methods for isolation of biologically active compounds from environmental samples. The procedures are applied to the determination of these analytes using spectrophotometric and chromatographic methods with different kinds of detection. Professor BARBARA STARCZEWSKA works at Institute of Chemistry (Biological–Chemical Department, University of Bialystok). Her studies are relative to elaboration of new extraction procedures for isolation of organic compounds from food and environmental samples. The techniques are applied to the determination of analytes using liquid chromatography method with different kinds of detection (especially connected with tandem mass spectrometry). Professor JOANNA KARPIŃSKA works at Institute of Chemistry (Biological–Chemical Department, University of Bialystok). Her studies are relative to elaboration of new microextraction techniques for isolation of organic compounds from environmental samples. The procedures are applied to the determination of analytes using gas chromatography and liquid chromatography methods with different kinds of detection (especially connected with tandem mass spectrometry). MONIKA KASABUŁA studies at Institute of Chemistry (Biological–Chemical Department, University of Bialystok) and her studies were relative to elaboration of micellar extraction for isolation of antihistaminic drugs from surface water samples and their determination using spectrophotometric and chromatographic methods with different kinds of detection. |
| E-mail: | Ilona Kiszkiel-Taudul: i.kiszkiel@uwb.edu.pl |
| Sponsorzy: | This work was financially supported by the Ministry of Science and Higher Education (Grant: NN305189435). Author Ilona Kiszkiel-Taudul was a beneficiary of the project Scholarships for PhD students of Podlaskie Voivodeship. The project was co-financed by European Social Fund, Polish Government and Podlaskie Voivodeship. |
| URI: | http://hdl.handle.net/11320/16409 |
| DOI: | 10.1007/s11743-017-2003-3 |
| ISSN: | 1097-3958 |
| e-ISSN: | 1558-9293 |
| Typ Dokumentu: | Article |
| metadata.dc.rights.uri: | https://creativecommons.org/licenses/by/4.0/ |
| Właściciel praw: | Creative Commons Attribution 4.0 International License |
| Występuje w kolekcji(ach): | Artykuły naukowe (WChem) |
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| Plik | Opis | Rozmiar | Format | |
|---|---|---|---|---|
| I_Kiszkiel_Taudul_B_Starczewska_J_ Karpinska_M_Kasabula_Application_of_Micellar_Extraction_for_Isolation_of_Famotidine.pdf | 649,23 kB | Adobe PDF | Otwórz |
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