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Tytuł: Fast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budget
Autorzy: Leśniewska, Barbara
Kisielewska, Katarzyna
Wiater, Józefa
Godlewska-Żyłkiewicz, Beata
Słowa kluczowe: Sequential extraction
Modified BCR procedure
Zinc fractions
Ultrasound probe
Uncertainty budged
Data wydania: 2016
Data dodania: 26-maj-2023
Wydawca: Springer
Źródło: Environmental Monitoring and Assessment, Volume 188, Issue 1 (2016), p. 1-13
Abstrakt: A new fast method for determination of mobile zinc fractions in soil is proposed in this work. The three-stage modified BCR procedure used for fractionation of zinc in soil was accelerated by using ultrasounds. The working parameters of an ultrasound probe, a power and a time of sonication, were optimized in order to acquire the content of analyte in soil extracts obtained by ultrasound-assisted sequential extraction (USE) consistent with that obtained by conventional modified Community Bureau of Reference (BCR) procedure. The content of zinc in extracts was determined by flame atomic absorption spectrometry. The developed USE procedure allowed for shortening the total extraction time from 48 h to 27 min in comparison to conventional modified BCR procedure. The method was fully validated, and the uncertainty budget was evaluated. The trueness and reproducibility of the developed method was confirmed by analysis of certified reference material of lake sediment BCR-701. The applicability of the procedure for fast, low costs and reliable determination of mobile zinc fraction in soil, which may be useful for assessing of anthropogenic impacts on natural resources and environmental monitoring purposes, was proved by analysis of different types of soil collected from Podlaskie Province (Poland).
Afiliacja: Barbara Leśniewska - University of Bialystok, Institute of Chemistry, Bialystok, Poland
Katarzyna Kisielewska - University of Bialystok, Institute of Chemistry, Bialystok, Poland
Józefa Wiater - Bialystok University of Technology, Faculty of Civil and Environmental Engineering, Bialystok, Poland
Beata Godlewska-Żyłkiewicz - University of Bialystok, Institute of Chemistry, Bialystok, Poland
E-mail: Barbara Leśniewska:
DOI: 10.1007/s10661-015-5020-6
ISSN: 0167-6369
e-ISSN: 1573-2959
Typ Dokumentu: Article
Właściciel praw: ©The Author(s) 2015. This article is published with open access at
This article is distributed under the terms of the Creative Commons Attribution 4.0 International License, which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.
Występuje w kolekcji(ach):Artykuły naukowe (WChem)

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