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    • Proszę używać tego identyfikatora do cytowań lub wstaw link do tej pozycji: http://hdl.handle.net/11320/15013
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    Pole DCWartośćJęzyk
    dc.contributor.authorLeśniewska, Barbara-
    dc.contributor.authorKisielewska, Katarzyna-
    dc.contributor.authorWiater, Józefa-
    dc.contributor.authorGodlewska-Żyłkiewicz, Beata-
    dc.date.accessioned2023-05-26T08:53:18Z-
    dc.date.available2023-05-26T08:53:18Z-
    dc.date.issued2016-
    dc.identifier.citationEnvironmental Monitoring and Assessment, Volume 188, Issue 1 (2016), p. 1-13pl
    dc.identifier.issn0167-6369-
    dc.identifier.urihttp://hdl.handle.net/11320/15013-
    dc.description.abstractA new fast method for determination of mobile zinc fractions in soil is proposed in this work. The three-stage modified BCR procedure used for fractionation of zinc in soil was accelerated by using ultrasounds. The working parameters of an ultrasound probe, a power and a time of sonication, were optimized in order to acquire the content of analyte in soil extracts obtained by ultrasound-assisted sequential extraction (USE) consistent with that obtained by conventional modified Community Bureau of Reference (BCR) procedure. The content of zinc in extracts was determined by flame atomic absorption spectrometry. The developed USE procedure allowed for shortening the total extraction time from 48 h to 27 min in comparison to conventional modified BCR procedure. The method was fully validated, and the uncertainty budget was evaluated. The trueness and reproducibility of the developed method was confirmed by analysis of certified reference material of lake sediment BCR-701. The applicability of the procedure for fast, low costs and reliable determination of mobile zinc fraction in soil, which may be useful for assessing of anthropogenic impacts on natural resources and environmental monitoring purposes, was proved by analysis of different types of soil collected from Podlaskie Province (Poland).pl
    dc.language.isoenpl
    dc.publisherSpringerpl
    dc.rightsUznanie autorstwa 4.0 Międzynarodowe*
    dc.rights.urihttp://creativecommons.org/licenses/by/4.0/*
    dc.subjectSequential extractionpl
    dc.subjectModified BCR procedurepl
    dc.subjectZinc fractionspl
    dc.subjectUltrasound probepl
    dc.subjectUncertainty budgedpl
    dc.titleFast and simple procedure for fractionation of zinc in soil using an ultrasound probe and FAAS detection. Validation of the analytical method and evaluation of the uncertainty budgetpl
    dc.typeArticlepl
    dc.rights.holder©The Author(s) 2015. This article is published with open access at Springerlink.compl
    dc.rights.holderThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License, which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.pl
    dc.identifier.doi10.1007/s10661-015-5020-6-
    dc.description.EmailBarbara Leśniewska: blesniew@uwb.edu.plpl
    dc.description.AffiliationBarbara Leśniewska - University of Bialystok, Institute of Chemistry, Bialystok, Polandpl
    dc.description.AffiliationKatarzyna Kisielewska - University of Bialystok, Institute of Chemistry, Bialystok, Polandpl
    dc.description.AffiliationJózefa Wiater - Bialystok University of Technology, Faculty of Civil and Environmental Engineering, Bialystok, Polandpl
    dc.description.AffiliationBeata Godlewska-Żyłkiewicz - University of Bialystok, Institute of Chemistry, Bialystok, Polandpl
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    dc.identifier.eissn1573-2959-
    dc.description.volume188pl
    dc.description.issue1pl
    dc.identifier.citation2Environmental Monitoring and Assessmentpl
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