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    • Proszę używać tego identyfikatora do cytowań lub wstaw link do tej pozycji: http://hdl.handle.net/11320/15016
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    Pole DCWartośćJęzyk
    dc.contributor.authorLeśniewska, Barbara-
    dc.contributor.authorKrymska, Marta-
    dc.contributor.authorŚwierad, Ewelina-
    dc.contributor.authorWiater, Józefa-
    dc.contributor.authorGodlewska-Żyłkiewicz, Beata-
    dc.date.accessioned2023-05-29T08:04:26Z-
    dc.date.available2023-05-29T08:04:26Z-
    dc.date.issued2016-
    dc.identifier.citationEnvironmental Science and Pollution Research, Volume 23, Issue 24 (2016), p. 25093–25104pl
    dc.identifier.urihttp://hdl.handle.net/11320/15016-
    dc.description.abstractA fast ultrasound-assisted sequential extraction (UASE) procedure for the determination of cadmium, lead and nickel fractions in soil was developed and fully validated. The working parameters of an ultrasound probe were optimized by comparing the content of metals in soil extracts obtained by the UASE procedure with that obtained by the conventional (with the aid of a vertical rotor) modified Community Bureau of Reference (BCR) procedure. The content of metals in soil fractions was determined by electrothermal atomic absorption spectrometry. The total time of extraction of metals from soil was shorten from 48 h to 27 min (total sonication time). The trueness of the developed method was confirmed by analysis of the certified reference material BCR701. In order to indicate critical points of the developed UASE method, uncertainties of fractionation results were calculated and compared with those calculated for conventional modified BCR procedure. The method usefulness was tested for the determination of metal fractions in different types of soil collected in the Podlasie Province (Poland). The proposed procedure could be used for fast screening of mobile fractions of several heavy metals in soil.pl
    dc.language.isoenpl
    dc.publisherSpringerpl
    dc.rightsUznanie autorstwa 4.0 Międzynarodowe*
    dc.rights.urihttp://creativecommons.org/licenses/by/4.0/*
    dc.subjectUltrasound probepl
    dc.subjectModified BCR sequential extractionpl
    dc.subjectEnvironmental analysispl
    dc.subjectUncertainty budgetpl
    dc.titleAn ultrasound-assisted procedure for fast screening of mobile fractions of Cd, Pb and Ni in soil. Insight into method optimization and validationpl
    dc.typeArticlepl
    dc.rights.holder© The Author(s) 2016. This article is published with open access at Springerlink.compl
    dc.rights.holderThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http:// creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were madepl
    dc.identifier.doi10.1007/s11356-016-7745-3-
    dc.description.EmailBarbara Leśniewska: blesniew@uwb.edu.plpl
    dc.description.AffiliationBarbara Leśniewska - Institute of Chemistry, University of Bialystok, Białystok, Polandpl
    dc.description.AffiliationMarta Krymska - Institute of Chemistry, University of Bialystok, Białystok, Polandpl
    dc.description.AffiliationEwelina Świerad - Institute of Chemistry, University of Bialystok, Białystok, Polandpl
    dc.description.AffiliationJózefa Wiater - Faculty of Civil and Environmental Engineering, Bialystok University of Technology, Białystok, Polandpl
    dc.description.AffiliationBeata Godlewska-Żyłkiewicz - Institute of Chemistry, University of Bialystok, Białystok, Polandpl
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    dc.identifier.eissn1614-7499-
    dc.description.volume23pl
    dc.description.issue24pl
    dc.identifier.citation2Environmental Science and Pollution Researchpl
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